Dewatering process

Distillation: processes – separatory – Distilling to separate or remove only water – From organic compound

Reexamination Certificate

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Details

C203S057000, C203S060000, C203S061000, C203S099000, C203SDIG019, C203SDIG021, C568S492000, C568S493000

Reexamination Certificate

active

07338579

ABSTRACT:
A formaldehyde-containing product is separated from a formalin solution containing formaldehyde, water, and methanol by distilling in the presence of a water entraining compound, especially methyl propionate or methyl methacrylate. The product contains substantially less water than in the solution and may be used, for example, in a further process which requires a source of formaldehyde containing a relatively low level of water, for example, the catalyzed reaction of methy propionate with formaldehyde and methanol to produce methyl methacrylate.

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The Chemical Hanbook, Basic Edition, 3rdVersion, 1984, Section II, pp. 144-145. (Partial English Translation attached).
The Solvent Handbook, 1985, 6thPrinting, pp. 589. (Partial English Translation attached).

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