Device for coupling a microchromatograph with a mass...

Measuring and testing – Gas analysis – Gas chromatography

Reexamination Certificate

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C073S023420, C095S087000, C096S106000, C422S089000

Reexamination Certificate

active

06907768

ABSTRACT:
A coupling device connecting the output of a microchromatograph (μCG) to the input of a mass spectrometer (MS), said coupling device comprising a capillary tube with one end connected in sealed fashion to the source under vacuum of the mass spectrometer through the intermediary of an interface device, and with the other end connected to the output of the microchromatograph, in slack fashion, open to the atmosphere; the length and the diameter of the capillary tube being chosen such that the flow rate inside the capillary tube is very close to the flow rate at the output from the microchromatograph; the interface device being, furthermore, provided with heating means for very precise adjustment of the flow rate registered by the capillary.

REFERENCES:
patent: 4662914 (1987-05-01), Hansen et al.
patent: WO 97/23779 (1997-07-01), None
XP-000993588 Henneberg, et al., “High-Performance Gas Chromatograph-Mass Spectrometer Interfacing: Investigation and Optimization of Flow and Temperature”, Journal of Chromatography, 167, pp. 139-147 (1978).
XP-000993587 Henneberg, et al., “Special Techniques in the Combination of Gas Chromatography and Mass Spectrometry”, Journal of Chromatography, 112, pp. 343-352 (1975).
Message, “Practical Aspects of gas chromatography/mass spectrometry”, John Wiley & Sons ed., (1984) (abstract only).

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