Device for analyzing samples for mercury and/or hydride-forming

Chemical apparatus and process disinfecting – deodorizing – preser – Analyzer – structured indicator – or manipulative laboratory... – Means for analyzing liquid or solid sample

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422 83, 422 91, 436 81, C01G 1300

Patent

active

050986589

ABSTRACT:
In a device for analyzing samples for mercury and/or hydride-forming elements by means of atomic absorption spectroscopy, a first arrangement for determining the mercury according to the amalgam method comprising passage throttling means in the form of a washing bottle and a tube connected downstream to a reaction vessel, the other end of which tube is connected to the measuring cell. The tube contains a gold net adapted to be heated and recooled according to the amalgam method. The second arrangement by which hydrides of the sample are directly connected to the measuring cell employs a conduit which leads directly to the measuring cell, bypassing the gold net by branching off from between the reaction vessel and washing bottle. The tube is connectable to a carrier gas source between the washing bottle and position of the gold net in the tube through a first shut-off valve. A second shut-off valve is arranged in the conduit directly leading to the measuring cell. The first and the second shut-off valves are interconnected so that opening the first shut-off valve causes the second shut-off valve to close.

REFERENCES:
patent: 3711248 (1973-01-01), Coffey
patent: 3713776 (1973-01-01), Capuano
patent: 3826614 (1974-07-01), Capuano
patent: 3826618 (1974-07-01), Capuano
patent: 3844719 (1974-10-01), Hammitt
patent: 3884639 (1975-05-01), Sugiyama
patent: 4023929 (1977-05-01), Becker et al.
patent: 4404288 (1983-09-01), Huber
patent: 4758519 (1988-07-01), Nakao et al.

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