Device and method for determining freezing points

Thermal measuring and testing – Transformation point determination – By thermal arrest

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374 16, G01N 2502

Patent

active

046015876

ABSTRACT:
A freezing point method and device (10) are disclosed. The method and device pertain to an inflection point technique for determining the freezing points of mixtures. In both the method and device (10), the mixture is cooled to a point below its anticipated freezing point and then warmed at a substantially linear rate. During the warming process, the rate of increase of temperature of the mixture is monitored by, for example, thermocouple (28) with the thermocouple output signal being amplified and differentiated by a differentiator (42). The rate of increase of temperature data are analyzed and a peak rate of increase of temperature is identified. In the preferred device (10) a computer (22) is utilized to analyze the rate of increase of temperature data following the warming process. Once the maximum rate of increase of temperature is identified, the corresponding temperature of the mixture is located and earmarked as being substantially equal to the freezing point of the mixture. In a preferred device (10), the computer (22), in addition to collecting the temperature and rate of change of temperature data, controls a programmable power supply (14) to provide a predetermined amount of cooling and warming current to thermoelectric modules (56).

REFERENCES:
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patent: 3319457 (1967-05-01), Leone
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patent: 3518838 (1970-07-01), Newton
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patent: 4383770 (1983-05-01), Boschung et al.
"Thermal Analysis", by T. Daniels, Kogan Page Ltd., 1973.
"Determination of the Purity of Hydrocarbons by Measurement of Freezing Points", A. R. Glascow, Jr. et al., U.S. Department of Commerce, National Bureau of Standards, 1945.

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