Detection of nitrate esters using silver electrode

Chemistry: electrical and wave energy – Processes and products

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G01N 2748

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044365900

ABSTRACT:
A method for the detection of nitrate esters using a solid working electrode of silver, copper, or gold. The method involves the forming of a test solution of a sample and supporting electrolyte, the insertion of the solution into a cell having the solid working electrode, deoxygenation of the test solution, application of a linearly varying potential to the cell and the recording of a voltammogram to show the reduction wave of the nitrate esters.

REFERENCES:
patent: 3922205 (1975-11-01), McLean et al.
D. A. Shaw et al., ISA Transactions, vol. 15, No. 3, pp. 227-232, (1976).
I. M. Kolthoff et al., "Polarography", vol. I, pp. 359-360, (1952).
M. H. Miles and D. A. Fine, J. Electroanal. Chem., vol. 127, 143-155 (198 ).

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