Detection of chloromethyl methyl ether or bis-chloro-methyl ethe

Details Detection of chloromethyl methyl ether or bis-chloro-methyl ethe Detection of chloromethyl methyl ether or bis-chloro-methyl ethe

1973-07-12

1976-03-16

Wolk, Morris O.

Chemistry: physical processes

Physical processes

Crystallization

23232C, 23230M, G01N 3108

Patent

active

039443892

ABSTRACT:
Method for quantitatively determining the presence of chloromethyl methyl ether and/or bis-chloromethyl ether in a fluid.
The above compounds are reacted with a reactant from the group consisting of an alkali metal salt of a lower alcohol, an alkali metal salt of phenol or an alkyl phenol, an alkali metal salt of a chlorophenol or bromophenol, an alkali metal salt of an alkoxy phenol, an alkali metal salt of a chlorinated pyridinol, and an alkali metal salt of thiophenol or a chlorinated thiophenol, dissolved in a lower alcohol, to form derivatives which provide suitable stability, specificity and sensitivity when applied to a gas chromatograph utilizing a suitable detector.

REFERENCES:
patent: 3807217 (1974-04-01), Wilkins et al.

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