Densification of carbon fiber preforms with pitches for...

Plastic and nonmetallic article shaping or treating: processes – Carbonizing to form article – With carbonizing – then adding carbonizable material and...

Reexamination Certificate

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C264S103000, C264S029100

Reexamination Certificate

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07897072

ABSTRACT:
Low cost isotropic and/or mesophase pitch is used to densify carbon fiber preforms by VPI and/or RTM equipment in place of CVI/CVD processing, for reduced manufacturing cycle times and costs and reduced need for expensive densification equipment. The process includes: heat treating a carbon fiber preform; infiltrating the preform with a pitch feedstock by VPI and/or RTM; carbonizing the pitch-infiltrated carbon fiber preform at 1200-2450° C. with a hold time of 4 hrs to ensure the entire furnace reaches the max temperature; repetition of the pitch infiltration and carbonization steps until the density of the preform is about 1.7 g/cc or higher; and a final heat-treatment of the densified composite. Brake discs manufactured in this way have higher densities and better thermal characteristics, which result in improved mechanical properties and friction and wear performance as compared with conventional CVI/CVD-densified brake discs.

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Extended European Search Report from corresponding EP Application No. 09 153 382.8, mailed Jul. 13, 2009, 5 pages.
European Examination Report from corresponding EP Application No. 09 153 382.8, mailed Jun. 1, 2010, 4 pages.

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