Metal treatment – Stock – Age or precipitation hardened or strengthened
Patent
1995-01-30
1997-02-25
Simmons, David A.
Metal treatment
Stock
Age or precipitation hardened or strengthened
148409, C22C 1905
Patent
active
056055846
ABSTRACT:
Columnar grain and single crystal nickel base superalloys are heat treated to provide a damage tolerant microstructure. The microstructure contains large, irregularly shaped "barrier" .gamma.' particles interspersed in an ordered array of smaller cuboidal .gamma.' particles in a .gamma. phase matrix. The barrier particles interrupt the progression of cracks through the microstructure. The invention process includes solutioning the .gamma.' phase, cooling slowly to a temperature about 50.degree. F. to 150.degree. F. (28.degree. C. to 83.degree. C.) below the .gamma.' solvus temperature, further cooling at a rate of at least about 100.degree. F. (56.degree. C.) per minute to less than 1000.degree. F. (538.degree. C.), reheating to 1975.degree. F. to 2000.degree. F. (1079.degree. C. to 1093.degree. C.) and holding for about four to six hours, cooling at 100.degree. F. (56.degree. C.) per minute to less than 1000.degree. F. (538.degree. C.), and heating to 1600.degree. F. .+-.25.degree. F. (871.degree. C. .+-.14.degree. C.) and holding for 24 hours to 32 hours.
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Cowles Bradford A.
DeLuca Daniel P.
Jones Howard B.
Phipps Margery S.
Simmons David A.
United Technologies Corporation
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