Cyanide-containing hemoglobin reagent composition and method pro

Chemistry: analytical and immunological testing – Hemoglobin – myoglobin – or occult blood

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436 8, 436 17, 436 18, 436 63, 436175, 435 2, 2524081, G01N 3372

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active

058587942

ABSTRACT:
The invention describes an improved stable reagent composition and method for the determination of hemoglobin (Hb) using whole blood samples and automated hematology analyzers. The Hb reagent contains an inorganic cyanide salt, at least one surfactant and a base and has a final pH of about 10.0 to about 11.2, preferably about 10.4 to about 11.2 or less and more preferably about 10.8 to about 11.2 or less. This reagent is intended for use as a universal Hb determination reagent for all of the instruments in the aforementioned series and will provide accurate and precise results without accompanying interference from elevated numbers of white blood cells, especially as found in abnormal blood specimens, and without system-to-system variation in the results obtained.

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M.J. Malin et al., 1989, "Evaluation of 24-Second Cyanide-Containing and Cyanide-Free Methods for Whole Blood Hemoglobin on the Technicon H*1.TM. Analyzer with Normal and Abnormal Blood Samples"; American Journal of Clinical Pathology, vol. 92, No. 3, pp. 286-294.
M.J. Malin and S.S. Fan, 1992, "Mechanism of automated alkaline methods for the determination of hemoglobin in whole blood based on the micellization of ligated heme in the presence and absence of cyanide"; Analytica Chimica Acta, 262:61-77.
T. Matsubara et al., 1972, "Proposal for an Improved Reagent in the Hemiglobincyanide Method"; Modern Concepts in Hematology, pp. 29-43.
B.A. Payne et al., 1986, "Evaluation of the TOA E-5000.RTM. Automated Hematology Analyzer"; Dept. of Laboratory Medicine, Mayo Clinic and May Foundation, Rochester, Minnesota, pp. 51-57.
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