Crystallization process

Refrigeration – Processes – Fractionally solidifying a constituent and separating the same

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62535, 62537, 62539, 62540, 62542, 23295R, 422251, B01D 900

Patent

active

046233725

ABSTRACT:
An improved crystallization process is disclosed for separating a crystallizable material and an excluded material which is at least partially excluded from the solid phase of the crystallizable material obtained upon freezing a liquid phase of the materials. The solid phase is more dense than the liquid phase, and it is separated therefrom by relative movement with the formation of a packed bed of solid phase. The packed bed is continuously formed adjacent its lower end and passed from the liquid phase into a countercurrent flow of backwash liquid. The packed bed extends through the level of the backwash liquid to provide a drained bed of solid phase adjacent its upper end which is melted by a condensing vapor.

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Chemical Engineering, May 7, 1979, pp. 72-82, James A. Heist.
Rudd, Powers & Sirola, "Process Synthesis", pp. 259-280 (1973).
Scientific American, Dec. 1962, pp. 41-47.

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