Crystalline form of D-gulose

Sugar – starch – and carbohydrates – Products – Sugars only

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127 58, 127 60, C13F 300, C13F 1300, C13F 102

Patent

active

052155919

ABSTRACT:
Free flowing, substantially pure, non-hygroscopic, crystalline .beta.-D-gulopyranose is disclosed. This crystalline form of D-gulose is characterized by a sharp melting point of 130.degree.-132.degree. C., a specific optical rotation of -40.degree. and characteristic mutarotation. A method for preparation of crystalline .beta.-D-gulopyranose from D-gulose syrup is also disclosed. This method involves dilution of the D-gulose syrup, followed by initiation of crystallization, and isolation of .beta.-D-gulopyranose crystals. Crystalline .beta.-D-gulopyranose may be used as an excipient, a chelating agent, a pharmaceutical intermediate, a cleaning agent for glass and metals, a food additive, and as an additive for detergents.

REFERENCES:
patent: 3454425 (1969-07-01), Smythe et al.
patent: 3607392 (1971-09-01), Lauer et al.
patent: 4421568 (1983-12-01), Huibers
patent: 4963382 (1990-10-01), Arena et al.

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