Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose

Details Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose

1980-12-04

1982-08-10

Golian, Joseph M.

Organic compounds -- part of the class 532-570 series

Organic compounds

Carbohydrates or derivatives

426658, 426548, C07H 304, C07H 502

Patent

active

043439349

ABSTRACT:
Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose exists as the orthorhombic anhydrous form and as the pentahydrate, both of which are more stable than amorphous TGS. Crystals are obtained from seeded aqueous solutions, above 38.degree. C. for the anhydrate; below 38.degree. C. for the pentahydrate.

REFERENCES:
Lee et al., Structural Functions of Taste in the Sugar Series: Binding Characteristics of Disaccharides, J. Sci. Fd. Agric. 1975,26 15137521.
Kirk-Othmer Encyclopedia of Chemical Technology, 3rd Ed., 1979, vol. 7, John Wiley & Sons: New York, pp. 243-285.
Hough, Selective Replacement of Hydroxyl Groups in Sucrose, Abstract 55, American Chemical Society Division of Carbohydrate Chemistry 172nd ACS National Meeting, San Francisco, Ca., Aug. 30-Sep. 2, 1976.

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