Controlled synthesis of nanoparticles using continuous...

Chemistry of inorganic compounds – Selenium or tellurium or compound thereof – Binary compound

Reexamination Certificate

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C423S561100, C423S566100, C423S592100, C423S604000, C423S606000, C423S618000, C423S633000, C423S594190, C423S622000, C977S773000, C977S774000, C977S775000, C977S811000, C977S824000

Reexamination Certificate

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07811543

ABSTRACT:
A method and apparatus for producing surface stabilized nanometer-sized particles includes the steps of mixing reactants, a surface-stabilizing surfactant, and a high boiling point liquid to form a mixture, continuously passing the mixture through an ultrasonic spray nozzle to form a mist of droplets of the mixture, injecting the mist directly into a furnace to cause a reaction between species of the mixture, and collecting the nanometer-sized products. The ultrasonic nozzle is positioned directly at one end of the heating furnace, preferably the top end, for travel of the droplets through the furnace. The continuous liquid-flow process, along with certain operating parameters, eliminates the need for dilution of the high boiling point liquid with a low boiling point solvent as in the prior art, significantly increases the yield, improves the quality of the product, and makes the process scalable.

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