Controlled crystallization diperoxyacid process

Details Controlled crystallization diperoxyacid process Controlled crystallization diperoxyacid process

1981-01-19

1982-06-29

Lone, Werren B.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

568566, C07C17915

Patent

active

043372139

ABSTRACT:
Diperoxyacids are unstable compounds, and processes for their production have normally provided relatively low product throughputs per reactor vessel volume. The present invention is a method for making diperoxyacids in which formation of the diperoxyacids is controlled and a high solids throughput may be achieved. The inventive method includes a controlling step wherein a reaction solids phase is maintained at not greater than about 36 wt. % of a reaction system, more preferably maintained at about 12 wt. % to about 36 wt. %.

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patent: 3547597 (1970-05-01), Hays
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W. E. Parker, Journal of the American Chemical Society, Apr. 1957, p. 1929.
Organic Peroxides, vol. 1, Daniel Swern Editor, May 1970, p. 388.

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