Continuous process for phosphorylating starch

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbohydrates or derivatives

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536 49, 536108, 536110, C08B 3102

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active

042163102

ABSTRACT:
Starch is phosphorylated by a virtually pollution-free, continuous process whereby an aqueous reagent solution of a tripolyphosphate, orthophosphate or pyrophosphate salt or a mixture thereof is sprayed onto a moist starch cake on a rotary vacuum filter in an amount sufficient to achieve efficient impregnation of the starch cake without losing significant levels of salt to the effluent. In a preferred embodiment, the reagent solution contains alkali metal tripolyphosphate salt and is obtained by diluting a concentrated solution thereof. The thus-impregnated starch is subsequently dried and heat-reacted by known procedures to produce an orthophosphate starch monoester.

REFERENCES:
patent: 2806026 (1967-09-01), Evans
patent: 2824870 (1958-02-01), Neukom
patent: 2884413 (1959-04-01), Kerr et al.
patent: 3132066 (1964-05-01), Kerr et al.
patent: 3459632 (1969-08-01), Caldwell et al.
patent: 3793310 (1974-02-01), Elizer
patent: 4166173 (1979-08-01), Wurzburg et al.

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