Continuous process and system for production of glycidyl...

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

Reexamination Certificate

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C549S555000, C549S560000, C525S406000, C525S410000, C528S403000, C528S408000, C528S420000

Reexamination Certificate

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06870061

ABSTRACT:
A continuous and scalable process for producing glycidyl nitrate, or glyn, from glycerin, nitric acid, and caustic wherein the process includes the reaction of glycerin and nitric acid to form dinitroglycerin and the reaction of dinitroglycerin with caustic, such as sodium hydroxide, system for producing the inventive material is also disclosed. The vessel, a second reaction vessel, and a separation apparatus.

REFERENCES:
patent: 5120827 (1992-06-01), Willer et al.
patent: 5136062 (1992-08-01), Millar et al.
patent: 5145974 (1992-09-01), Paul et al.
patent: 6362311 (2002-03-01), Highsmith et al.
patent: WO 0129111 (2001-04-01), None
UK Patent Office Search Report dated Jun. 18, 2004.
French Patent Office Search Report dated Aug. 26, 2004.
Naoum, Phokion, Nitroglycerine and Nitroglycerine Explosives. The World Wide Chemical Translation Series. 1928, pp. 161-179, Number One. The Williams & Wilkins Company, Baltimore.
Urbanski, Tadeusz, Chemistry and Technology of Explosives. date unknown, pp. 90-140, vol. 2. Pergamon Press, Oxford, 1965.

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