Continuous preparation of nitrosyl fluoride

Chemistry of inorganic compounds – Nitrogen or compound thereof – Oxygen containing

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C01B 21084

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active

049082701

ABSTRACT:
A process and apparatus for the continuous production of nitrosyl fluoride from nitrite and hydrogen fluoride. Nitrite solids and hydrogen fluoride are separately introduced and blended into nitrosyl fluoride so as to form a reaction mixture within which the nitrite and the hydrogen fluoride react to produce additional nitrosyl fluoride. The hydrogen fluoride is introduced into the reaction mixture spaced away from where the nitrite is introduced into the reaction mixture so that the hydrogen fluoride and the nitrite separately mix into the nitrosyl fluoride and are diluted therein before mixing with each other, thereby avoiding a violent reaction between the hydrogen fluoride and the nitrite.

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