Continuous preparation of hydroxylammonium salts

Chemistry of inorganic compounds – Nitrogen or compound thereof – Oxygen containing

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423388, C01B 2120

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active

044774249

ABSTRACT:
An improved process for the continuous preparation of hydroxylammonium salts by catalytic reduction of nitric oxide with hydrogen in a dilute aqueous solution of a mineral acid in the presence of a suspended noble metal catalyst at an elevated temperature in several reaction zones connected in series, wherein the improvement comprises maintaining a pH of <2.0 in the last reaction zone.

REFERENCES:
patent: 4048291 (1977-09-01), El-Ghatta et al.
patent: 4192856 (1980-03-01), Rapp et al.

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