Continuous preparation of dialkanesulfonyl peroxide

Details Continuous preparation of dialkanesulfonyl peroxide Continuous preparation of dialkanesulfonyl peroxide

1986-11-03

1987-07-14

Demers, Arthur P.

Chemistry: electrical and wave energy

Processes and products

204 78, 568 28, C25B 302

Patent

active

046800956

ABSTRACT:
Dialkanesulfonyl peroxide (RSO.sub.2 --O--O--O.sub.2 SR) is prepared in a continuous process by electrolyzing the corresponding alkanesulfonic acid at an elevated temperature (to keep the peroxide product in solution) in a continuous-flow electrolysis cell, removing the solution from the electrolytic cell, cooling the solution to precipitate the peroxide product, and recycling the supernatant alkanesulfonic acid back to the cell.

REFERENCES:
patent: 2619507 (1952-11-01), Jones et al.
Heszeldine et al., J. Chem. Soc. (A), (1964) pp. 4901-4907.
Myall et al., J. Chem. Soc. (Penkins), (1975) pp. 953-955.

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