Continuous method for preparation of granulated sodium perborate

Chemistry of inorganic compounds – Boron or compound thereof – Oxygen containing

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23313R, 23313FB, 159 481, C01B 1512

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049685007

ABSTRACT:
The spray drying of a solution containing hydrogen peroxide and sodium metaborate to obtain primary particles which are immediately conveyed after leaving the drying zone to a granulating device and are then granulated in the presence of free and/or perborate water of crystallization. The granulated materials are dried, if necessary. The generally amorphous primary particles are converted into granulated materials with at least partially crystalline structure and significantly improved shelf life. The work is performed with advantage in a spray dryer with integrated fluid bed or in a compressing granulating device. The method is suitable for preparing perborate granulated materials with over 10% by wt., especially perborate monohydrate granular materials with 14-16% by wt. active oxygen.

REFERENCES:
patent: 3555696 (1971-01-01), Pistor et al.
patent: 4002434 (1977-01-01), Simmersbach et al.
patent: 4115519 (1978-09-01), Brichard et al.
patent: 4185960 (1980-01-01), Brichard et al.
patent: 4215097 (1980-07-01), Brichard et al.
patent: 4681748 (1987-07-01), Doetsch et al.

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