Continuous method and heat pump device for enriching liquid...

Chemistry of hydrocarbon compounds – Purification – separation – or recovery – By plural serial diverse separations

Reexamination Certificate

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C585S643000, C203S026000, C159S024100, C159S024200, C159S024300

Reexamination Certificate

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06906234

ABSTRACT:
A continuous method and a heat pump device for enrichment of low-concentrated reaction mixtures resulting from the production of cycloalkanedienes by means of catalytic metathesis of cyclic aliphatic alkenes and cyclooligomers in organic reaction media with reduced energy consumption. Using the heat pump principle, liquid reaction mixtures with a content of at least 0.1 w/w % are enriched in an organic reaction medium to 30 to 50 w/w %. The organic reaction medium at temperature T1is evaporated in an evaporator, the vapor is withdrawn and compressed to temperature T2in a compressor, at a pressure difference of 0.25 to 1 bar. Compressed vapor of the reaction medium transfers heat energy obtained from electric energy in the heat exchanger of the evaporator to the organic reaction medium at temperature T1, and the temperature difference (T2−T1) does not exceed 12 K.

REFERENCES:
patent: 343437 (1989-11-01), None
patent: 1105565 (1998-03-01), None

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