Continuous crystallization process

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

Reexamination Certificate

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Reexamination Certificate

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07034191

ABSTRACT:
A continuous crystallization process comprising the steps of supplying a crystallization material containing bisphenol A to a crystallizer to form crystals of an adduct of bisphenol A and phenol or crystals of bisphenol A, subjecting the slurry discharged from the crystallizer to solid/liquid separation, and recovering the crystals, wherein part of the mother liquor is circulated to the crystallizer. According to this process, the heat duty to be removed is reduced, deposition of solids on the inner surfaces of the crystallizer, particularly on the heat transferring surface of the cooler is restrained, and consequently the continuous operating time of the apparatus is prolonged.

REFERENCES:
patent: 4927978 (1990-05-01), Buechele et al.
patent: 4950805 (1990-08-01), Iimuro et al.
patent: 5345000 (1994-09-01), Moriya et al.
patent: 6806394 (2004-10-01), Evitt et al.
patent: 0 332 203 (1989-09-01), None
patent: 0 522 700 (1993-01-01), None
patent: 0 558 214 (1993-09-01), None
patent: WO 91/05755 (1991-05-01), None
patent: WO 200240435 (2002-05-01), None

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