Continuous crystallization

Sugar – starch – and carbohydrates – Processes – Carbohydrate manufacture and refining

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23273R, 127 16, 159 44, 159 45, C13F 102, C13K 110, C13K 500, C13K 1100

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active

039817393

ABSTRACT:
A crystallizable solute is crystallized from a solution containing the same by introducing a solution of said solute into a first stage evaporative-crystallization zone together with seed solute crystals. Within the first stage evaporative-crystallization zone the solution is concentrated to yield a saturated first stage concentrate containing crystals of said solute. The crystals of said solute are substantially larger than said seed crystals and are suspended in a solution more concentrated with respect to said solute than the solution supplied to said first evaporative-crystallization zone. A stream of said first concentrate is removed from said first evaporative-crystallization zone and transferred to a second evaporative-crystallization zone for further concentration or crystallization of solute and for the production of solute crystals of increased size. There is continuously recovered from the second evaporative-crystallization zone a slurry having a total solute or solids content of about 86-94 percent by weight and containing the solute crystals of desired crystal size.

REFERENCES:
patent: 667850 (1901-02-01), McNeil
patent: 2587293 (1952-02-01), DeVries
patent: 3220883 (1965-11-01), Howard
patent: 3424221 (1969-01-01), Luce
patent: 3530924 (1970-09-01), Domning
patent: 3709731 (1973-01-01), Kingma

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