Continuous centrifuges

Details Continuous centrifuges Continuous centrifuges

2000-08-17

2003-02-18

Reifsnyder, David A. (Department: 1723)

Liquid purification or separation

Flow, fluid pressure or material level, responsive

Diverse sensing means

C210S369000, C210S377000, C210S380100, C210S391000, C494S036000, C127S019000

Reexamination Certificate

active

06521120

ABSTRACT:

The present invention relates to continuous centrifuges of the type comprising a rotating perforated drum or basket (hereinafter referred to as a “basket”), along whose inner peripheral wall a liquids/solids mix is caused to travel, with solids being discharged over the mouth of the rotating basket and liquids being collected via the basket perforations.
The separation of crystalline materials from liquid (for example, sugar crystals in molasses) may be made in a tapered, rotating and perforated basket. In the present state of the art the basket is conical with the straight sides subtending an angle in the range of 22° to 36° to separate sugar crystals—with angles larger or smaller used on some other products. The conical basket is usually of single angle throughout its length, although it is also known for the basket to have regions of two different basket angles. For example, U.S. Pat. No. 379,953 describes a centrifuge basket having two portions of different inclination so selected that they are greater than the greatest angle of slide of the solid phase that is to be separated by the centrifuge. WO95/21697 describes a centrifuge basket having two portions of different inclination corresponding respectively to a lower zone providing drainage and filtration and an upper zone providing drainage only.
FIG. 1
of the accompanying drawings shows a typical state of the art continuous centrifuge. The basket (
1
) is perforated (
2
) and lined with a screen (
3
) perforated with fine slots, the slot width being less than the minimum crystal dimension. The basket rotates about a vertical axis (
4
) driven by a motor (
5
) and belts (
6
). The massecuite (a mixture of crystals and mother liquid) (
7
) flows through a control valve mounted near the axis (
4
) into a feeding pot (
9
). The function of the pot is (a) to accelerate the massecuite to the rotational speed of the smaller diameter (
10
) of the basket and (b) to distribute the massecuite evenly around the periphery of the basket smaller diameter portion (
10
). The solids remain suspended in the liquid until deposited on screen (
3
) for separation to commence. The angle (
11
) of the basket is such that the massecuite and crystals migrate up the basket wall, the mother liquid flowing progressively through the slots in the screen (
3
) and basket perforations (
2
) as it is subjected to the increasing centrifugal force of rotation. The crystals remain on the slotted screen and slide to the largest diameter of the basket to be discharged over the lip (
12
). The outer casing (
13
) of the centrifuge and baffles (
14
) guide the separated liquid and crystals to outlets (
15
) and (
16
), respectively.
The efficiency of the separation achieved, usually measured by the proportion of the total liquid separated (a small amount of liquid being carried over by the solids), depends upon the time taken for the crystals to travel over the slotted area of the screen—referred to as the “residence time”. The longer the residence time the higher the separating efficiency.
FIG. 2
of the accompanying drawings shows, in an elementary way and omitting the effects of gravity, the frictional and rotational forces on a typical isolated crystal on the perforated screen (
3
).
In
FIG. 2
, the isolated crystal (
17
) of unit mass is at radius r in conical basket (
1
) of angle &THgr; and rotation w. The centrifugal force G applied to the crystal is resolved into force x pushing the crystal up the basket and force y normal to the basket wall. The frictional force F between the crystal and basket wall that resists the movement of the crystal is &mgr;. y, where &mgr; is the coefficient of friction. From the geometry of
FIG. 2
, for the crystal to move to discharge, x must be greater than &mgr;.y. For an acceptable residence time then, tan &THgr; must be slightly greater than &mgr;.
Changes in the characteristics of the solid/liquid mixture as it moves up the screen during separation reduce the efficiency and residence time of the centrifuge described above. As the massecuite flows over the separating zone of the basket it passes through the stages described hereinafter and shown in
FIG. 3
of the accompanying drawings. (In this figure the dimensions of the flow are exaggerated to demonstrate the changes as separation proceeds).
Liquid stage (
18
).
The massecuite
3
A is subject to relatively low centrifugal force, much of the liquid remains in the basket and the flow is that of a liquid carrying individual free solids. The flow through this zone is streamlined with increasing viscosity as the liquid content is reduced, the viscosity being the main factor in controlling the flow rate.
Intermediate stage (
19
).
As the centrifugal force increases, more liquid is separated and some crystals make contact with others, with the interstices between them being filled with liquid. The crystals then slide on the screen (
3
), lubricated by the outward flow of inter-crystalline liquid. Both liquid viscosity and coefficients of friction between crystals (
17
) and screen (
3
) control the flow rate. During this stage, crystals appear on the surface of the liquid.
Solids stage (
20
).
Under high centrifugal force, the solids approaching discharge will behave either independently or as an interconnected mass. In the former, the solids volume is low and the solids are not in contact with each other. They slide independently to discharge, the sliding rate depending primarily upon the crystal (
17
) to screen (
3
) coefficient of friction. In the latter, a higher solids volume causes the crystals to be in contact with each other. Then the sliding rate to discharge will depend also on the inter-crystalline friction and any compaction or deformation of the crystals. This additional intercrystalline friction reduces the velocity of the crystals along the basket wall and increases the crystal residence time.
Wash stage (
21
).
On some applications, an additional liquid is applied near the junction of stages (
19
) and (
20
) and/or (
18
) and (
19
) to assist separation. This displaces some of the remaining mother liquid, washes the crystals and alters the viscosity locally.
In practice, there is a smooth transition between stages (
18
), (
19
) and (
20
) and out of the wash stage (
21
). At the commencement of stage (
18
), the thickness t of the massecuite can be many times that of the crystal bed of stage (
20
), altering the apparent angle at the massecuite inner surface to assist flow.
The residence time in each of the stages described above depends upon the viscosity, crystal/liquid ratio, coefficient of friction between the screen and crystals, the interactions between adjacent crystals and centrifugal force. These vary between the stages and the angle of the straight-sided conical basket must be chosen to ensure that the crystals slide under the most difficult conditions in a selected one of the stages, for example stage (
20
). Residence time is then uncontrolled during the other separating stages resulting in reduced residence time and separating efficiency.
In accordance with a first aspect of the present invention, the residence time over each separating stage individually is controlled by selecting and setting the basket angle locally to suit the local values controlling the flow at that stage. By this means, a desired residence time can be achieved during all separating stages, the basket separating surface can be used fully and maximum separating efficiency achieved.
In accordance with a second aspect of the present invention, there is provided a continuous centrifuge of the type comprising a perforated basket of generally frusto-conical configuration which is adapted to rotate about a rotational axis and along whose inner peripheral wall a liquids/solids mix is caused to travel, with solids being discharged over the mouth of the rotating basket at its wider end and liquids being collected via the basket perforations, wherein the basket wall has at least three regions of different inclination relative to the basket rotational axis corresponding respe

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