Continuous acid washing of polymer resin with controlled meterin

Liquid purification or separation – Processes – Including controlling process in response to a sensed condition

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210 87, 210 93, 210 961, 210143, 210182, 210202, 210259, 210769, 210770, 210772, 210774, 210806, 364502, 422 62, 422110, 422135, 422138, 436 55, 525537, 528486, B01D 1712, C08F28300

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active

052098559

ABSTRACT:
A batch type process for purification of a polymer resin, in which a predetermined volume of acid is rapidly emptied and stirred into a fixed volume of polymer slurry for chemically treating impurities in the slurry, is converted to a continuous operation by supplying a substantially constant stream of polymer slurry and a controlled stream of acid to a mixing vessel. pH control of the polymer slurry required for effective purification of the polymer resin is achieved by manipulating the flow rate of the acid stream responsive to a feedforward control signal which operates in conjunction with a feedback signal. The feedforward signal is based on an upstream measurement of slurry flow rate to the mixing vessel and the feedback signal is based on a downstream pH measurement of slurry flowing from the mixing vessel.

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