Conjoint production of C-methyl triethylene diamine and allyl pi

Organic compounds -- part of the class 532-570 series – Organic compounds – Nitrogen attached directly or indirectly to the purine ring...

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Details

544351, 544404, C07D48708, C07D29502, C07B 3710, C07B 3506

Patent

active

047540362

ABSTRACT:
N-(hydroxypropyl) piperazine and/or N,N'-(dihydroxypropyl) piperazine can conjointly be converted to C-methyl-triethylenediamine and allyl piperazine with excellent conjoint yield and selectivity when using a catalyst composed of titania to which from about 0.5 to about 7 wt. % of phosphorus has been thermally chemically bonded in the form of phosphate linkages.

REFERENCES:
patent: 3285920 (1966-11-01), Muhlbauer
patent: 4588842 (1986-05-01), Vanderpool
patent: 4647664 (1987-03-01), Vanderpool

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