Color stabilization of amines

Distillation: processes – separatory – Addition of material to distilland to inhibit or prevent...

Reexamination Certificate

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Details

C203S038000, C203S059000, C203S078000, C564S497000

Reexamination Certificate

active

10456655

ABSTRACT:
The present invention concerns a process for providing tertiary amine products which are color-stable, and have a greatly reduced tendency to take on color during their storage. According to the invention, an ethyleneamine derivative is added to the distillation pot prior to or during the distillation of the tertiary amine product. Preferably, the ethyleneamine derivative has a higher boiling point than the desired tertiary amine product so as to preclude the ethyleneamine from distilling over with the tertiary amine.

REFERENCES:
patent: 3567779 (1971-03-01), Currier et al.
patent: 4567303 (1986-01-01), Boettger et al.
patent: 4609436 (1986-09-01), Bakkum
patent: 4731165 (1988-03-01), Niebruegge et al.
patent: 4766247 (1988-08-01), Ford et al.
patent: 4806229 (1989-02-01), Ferguson et al.
patent: 5663444 (1997-09-01), Melder et al.
patent: 4414879 (1995-11-01), None
patent: 0 028 555 (1983-06-01), None

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