Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing
Patent
1993-08-11
1995-03-21
Kumar, Shailendra
Organic compounds -- part of the class 532-570 series
Organic compounds
Amino nitrogen containing
564142, 564144, 564223, 564 2, C07C23305
Patent
active
053997603
ABSTRACT:
A method is provided for purifying crude N-acetyl-para-aminophenol (APAP) containing color bodies or their precursors, the method comprising: a) forming a solution of the crude APAP; and b) subsequently contacting the solution with substoichiometric quantifies of an acetylating agent for a sufficient period of time to convert said color bodies or their precursors to substantially non-color bodies/stable, colorless substances; said quantities of acetylating agent provided is such that substantially none of the APAP is converted to other compounds.
REFERENCES:
patent: 3113150 (1963-12-01), Young
patent: 3748358 (1973-07-01), Baron
patent: 4524217 (1985-06-01), Davenport et al.
patent: 4607125 (1986-08-01), Mott
patent: 5155269 (1992-10-01), Dunn et al.
Merck Index, 10th Edition, 5135, p. 761, 1983.
Fruchey Olan S.
Lindley Daniel D.
Shockley Thomas H.
Trevino Joe S.
Wood B. Frank
Cassady Donald R.
Hoechst Celanese Corporation
Kumar Shailendra
Mullen James J.
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