Coal deashing process having improved solvent recovery technique

Mineral oils: processes and products – Phenolic or toxic oils

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C10G 100

Patent

active

041629566

ABSTRACT:
An improved coal deashing process wherein coal is mixed with a coal liquefaction process solvent, solubilized and flashed to provide a prepared mixture and the prepared mixture is mixed with a deashing solvent to produce a feed mixture. Thereafter, the feed mixture is separated in a first separation zone into a first heavy fraction comprising insoluble coal products and a first light fraction comprising soluble coal products and solvents. The first light fraction is recovered and a second portion of the deashing solvent is mixed with the first light fraction prior to introduction into a second separation zone wherein an improved separation occurs to produce a second light fraction comprising the solvents and a second heavy fraction comprising the soluble coal products which is recovered. The second light fraction is withdrawn and separated in a third separation zone into a third heavy fraction comprising the liquefaction process solvent for recycle to aid in solubilization of the coal and a third light fraction comprising the deashing solvent for recycle to aid in the production of the feed mixture.

REFERENCES:
patent: 3607716 (1971-09-01), Roach
patent: 3607717 (1971-09-01), Roach
patent: 3607718 (1971-09-01), Leaders et al.
patent: 3642608 (1972-02-01), Roach et al.
patent: 3852183 (1974-12-01), Snell
patent: 3856675 (1974-12-01), Sze et al.
patent: 4008054 (1977-02-01), Clancey et al.
patent: 4008145 (1977-02-01), Leas
patent: 4070268 (1978-01-01), Davis et al.

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