CO.sub.2 Pretreatment prevents calcium carbonate formation

Mineral oils: processes and products – Phenolic or toxic oils

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208 8R, 208 10, C10G 100, C10G 106

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active

042060338

ABSTRACT:
Scale formation during the liquefaction of lower ranking coals and similar carbonaceous materials is significantly reduced and/or prevented by pretreatment with carbon dioxide. The carbon dioxide pretreatment is believed to convert the scale-forming components to the corresponding carbonate prior to liquefaction. The pretreatment is accomplished at a total pressure within the range from about 14 to about 68 atmospheres and a carbon dioxide partial pressure within the range from about 14 to about 34 atmospheres. Temperature during pretreatment will generally be within the range from about 100.degree. to about 200.degree. C.

REFERENCES:
patent: 2191156 (1940-02-01), Pier et al.
patent: 2221410 (1940-11-01), Pier
patent: 3355376 (1967-11-01), Gorin et al.
patent: 3505204 (1970-04-01), Hoffman
patent: 3926775 (1975-12-01), Schroeder
patent: 4121910 (1978-10-01), Stambaugh
Def. Pub. Ser. No. 700,485 Pub. 4/22/69, Hemminger et al.

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