Chromatographic arylcarboxamide polysiloxanes

Liquid purification or separation – With means to add treating material – Chromatography

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2105021, 210656, 528 15, 528 23, 528 25, 528 42, 528 43, 556450, B01D 1508

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active

049099353

ABSTRACT:
Chiral arylcarboxamide-containing alkenes and alkoxysilanes and polysiloxane polymers containing chiral arylcarboxamide-substituted side chains and methods for their preparation are disclosed. The chiral arylcarboxamide-containing alkenes are used to prepare the chiral arylcarboxamide-containing polysiloxane polymers which are useful as stationary phase coatings in gas-liquid and supercritical fluid chromatography in the separation and analysis of enantiomeric and other stereoisomeric mixtures of various substances. The chiral arylcarboxamide containing alkoxysilanes are reactive towards silica particles for use as packing in liquid chromatography columns.

REFERENCES:
patent: 4745169 (1988-05-01), Sugiyama
Frank, "Rapid Gas-Chromatographic Separation of Amino-Acid Enantiomers with a Novel Chiral Stationary Phase", Journal of Chromatographic Science, 1977, vol. 15, pp. 174-179.
Richter, "Nonextractable Cyanopropyl Polysiloxane Stationary Phases for Capillary Chromatography," Chromatographia, 1983, vol. 17, pp. 570-573.
Kuei, N-Octylmethyl polysiloxane stationary phases for capillary gas and supercritical fluid chromatography Chromatographia, 1985, vol. 20, pp. 25-30.
Junes, "Synthesis at Smectic Liquid-Crystalline Polysiloxanes from Biphenyl Carboxylate Esters", Journal of Organic Chemistry, 1984, vol. 49, pp. 4947-4951.
W. A. Konig, "Separation of Enantiomers by Capillary Gas Chromatography with Chiral Stationary Phases" Journal of High Resolution Chromatography and Chromatography Communication, 1982, vol. 5, pp. 588-595.
Liu, "Chiral Stationary Phases for the Gas-Liquid Chromatographic Separation of Enantiomers" Journal of Chromatography, 1983, vol. 271, pp. 309-323.
Koppenhoefer, "Chiral Recognition in Gas Chromatographic Analysis of Enantiomers on Chiral Polysiloxanes," Journal of Chromatography Library, 1985, vol. 32 pp. 1-42.
Roder, Chiral SFC-Separations Using Polymer Coated Open Tubular Fused Silica Columns, Journal of High Resolution Chromatography and Chromatography Communications 1987, vol. 10, pp. 665-667.

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