Coating processes – Coating by vapor – gas – or smoke
Reexamination Certificate
2001-09-10
2004-09-21
Meeks, Timothy (Department: 1762)
Coating processes
Coating by vapor, gas, or smoke
C427S252000, C427S253000
Reexamination Certificate
active
06793966
ABSTRACT:
FIELD OF THE INVENTION
The present invention relates to a chemical vapor deposition (CVD) apparatus and method for applying coatings to substrates.
BACKGROUND OF THE INVENTION
Chemical vapor deposition (CVD) involves the generation of metal halide gas at low temperatures (e.g. about 100 to 600 degrees C.), introduction of the metal halide gas into a high temperature retort (e.g. 200 to 1200 degrees C. retort temperature), and reaction of the metal halide with substrates positioned in the retort to form a coating thereon. In general, a large excess of metal halide gas is used to prevent reactant starvation in the high temperature coating retort. CVD processes typically are conducted at reduced pressure (subambient pressure). CVD apparatus and method are described in Howmet U.S. Pat. Nos. 5,261,963 and 5,263,530. Howmet U.S. Pat. No. 6,143,361 described CVD apparatus and method wherein deposition of excess metal halide reactant in the coating gas exhausted from the coating retort is reduced or eliminated to reduce retort downtime required to remove deposits from the retort exhaust system.
The CVD process can be used to codeposit Al, Si, and one or more reactive elements such as Hf, Zr, Y, Ce, La, etc. to form protective aluminide diffusion coatings on substrates such as nickel and cobalt base superalloys commonly used to cast gas turbine engine airfoils. Copending U.S. Ser. Nos. 08/197,497 and 08/197 478 disclose CVD apparatus and method to produce protective reactive element-modified aluminide diffusion coatings. U.S. Pat. No. 5,989,733 describes a protective outwardly grown, platinum-modified aluminide diffusion coating containing Si and Hf and optionally Zr, Y, Ce, and/or La formed on a nickel or cobalt base superalloy substrate by such CVD apparatus and process.
There is a need to provide improved CVD apparatus and method that are capable of producing aluminide diffusion coatings modified by inclusion of one or more other coating elements, such as for example only silicon and one or more so-called reactive elements, wherein the coatings can be produced having a more uniform coating composition, microstructure, and thickness throughout the working volume (throughout multiple coating zones) of the CVD coating apparatus. It is an object of the present invention to satisfy this need.
SUMMARY OF THE INVENTION
In one embodiment of the present invention, CVD apparatus and method are provided with an improved coating gas distribution system to provide more uniform coating gas temperature among a plurality of coating zones in a coating chamber.
In another embodiment of the present invention, CVD apparatus and method are provided with an improved coating gas distribution system to provide more uniform flow of coating gas among a plurality of coating zones in the coating chamber.
In still another embodiment of the present invention, CVD apparatus and method are provided with an improved coating gas exhaust system that reduces interaction between the inlet coating gas flow to each coating zone and exhaust gas flow from each coating zone so as provide a more uniform gas flow pattern in each coating zone.
The above and other objects and advantages of the present invention will become more readily apparent from the following detailed description taken with the following drawings.
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Ser. No. 09/950,012 filed Sep. 10, 2001.
Near Daniel L.
Purvis Andrew L.
Warnes Bruce M.
Howmet Research Corporation
Meeks Timothy
Timmer Edward J.
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