Chemical synthesis of flavipucine

Details Chemical synthesis of flavipucine Chemical synthesis of flavipucine

1977-05-19

1978-06-13

Randolph, John D.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

424263, C07D21140

Patent

active

040948781

ABSTRACT:
A method for the total chemical synthesis of flavipucine employs the condensation of 4-hydroxy-6-methyl-2-pyridone with isobutylglyoxal in alkali alkoxide. The resulting alkali salt is acylated in both the 1' and 4 positions. Treatment of the 1',4-diacyloxy derivative with excess alkaline peroxide yields flavipucine.

REFERENCES:
girota et al., J. Chem. Soc., Chem. Comm. 1976, pp. 566 to 567.
Chemical Abstracts, vol. 77, abst. No. 114194m (1972) (abst. of Findlay et al., J. Chem. Soc., Perkin Trans. 1 1972, pp. 2071-2074).
Findlay et al., Can. J. Chem. vol. 54, pp. 270 to 274 (1976).
Findlay et al., Synthetic Communications, vol. 3, pp. 355-358 (1973).

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