Chemistry of inorganic compounds – Oxygen or compound thereof – Metal containing
Reexamination Certificate
2006-03-28
2006-03-28
Bos, Steven (Department: 1754)
Chemistry of inorganic compounds
Oxygen or compound thereof
Metal containing
C423S594400, C423S594600, C423S599000, C423S600000
Reexamination Certificate
active
07018607
ABSTRACT:
A method is disclosed for synthesizing a crystalline metal oxide powder material containing two or more uniformly distributed metal elements. Crystalline, water containing, oxygen containing inorganic acid salts of the metals are heated to liquefy the salts. The apparent solution contains a uniform mixture of the metal elements. The water is removed from the liquid and the resulting powder calcined in air to decompose the acid salts to a mixed metal crystalline oxide. The method is particularly useful to make doped LiNiO2type crystals using hydrated nitrate or nitrite salts of Li, Ni and the dopant elements. Examples of useful salts are LiNO3.H2O, Ni(NO3)2.6H2O, Co(NO3)2.6H2O, Al(NO3)3.9H2O, and Mg(NO3)2.6H2O.
REFERENCES:
patent: 5985488 (1999-11-01), Mitate et al.
patent: 6054110 (2000-04-01), Yamada et al.
patent: 6071489 (2000-06-01), Sun et al.
patent: 2003/0031930 (2003-02-01), Hamano et al.
Garabedian Gregory Charles
Nazri Gholam-Abbas
Bos Steven
General Motors Corporation
Marra Kathryn A.
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