Catalytic polymerization process

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Polymers from only ethylenic monomers or processes of...

Reexamination Certificate

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C526S073000, C526S079000, C526S140000, C526S319000, C526S329100, C526S346000

Reexamination Certificate

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07148297

ABSTRACT:
This invention relates to a process for controlling the architecture of copolymers of at least two unsaturated monomers, made by free-radical polymerization in the presence of a cobalt-containing chain transfer agent, including the control of molecular weight, degree of branching and vinyl end group termination, by varying at least one of the variables of molar ratio of monomers, their relative chain transfer constants, polymerization temperature and degree of conversion and amount of cobalt chain transfer agent; and polymers made thereby.

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Salamonczyk et al., J. Org. Chem. 1996, 61, pp. 6893-6900.
Kowollick et al., Evolution of MW distribution in the Catalytic Chain Transfer Polymerization of MMA up to high Monomer conversion, Polymer Science, Part A, 2000, vol. 38, p. 3303-3312.
Roberts G. E. et al.Macromolecules2000, vol. 33, 7765-7768.

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