Catalytic dewaxing of light and heavy oils in dual parallel reac

Mineral oils: processes and products – Chemical conversion of hydrocarbons – Plural parallel stages of chemical conversion

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Details

208 97, 208111, 208120, C10G 6518, C10G 6512, C10G 6702

Patent

active

046054880

ABSTRACT:
Relatively heavy and relatively light lube chargestocks are dewaxed in two parallel, separate reactors. The reactor used for dewaxing the relatively light chargestock contains a crystallize zeolite having pore openings defined by: (1) a ratio of sorption of n-hexane to o-xylene, on a volume percent basis, of greater than 3, which sorption is determined at a P/P.sub.o of 0.1 and at a temperature of 50.degree. C. for n-hexane and 80.degree. C. for o-xylene and (2) by the ability of selectively cracking 3-methylpentane (3MP) in preference to the doubly branched 2,3-dimethylbutane (DMB) at 1000.degree. F. and 1 atmosphere pressure from a 1/1/1 weight ratio mixture of n-hexane/3-methyl-pentane/2,3-dimethylbutane, with the ratio of rate constants k.sub.3MP /k.sub.DMB determined at a temperature of 1000.degree. F. being in excess of about 2, e.g., natural and synthetic ferrierite, ZSM-22, ZSM-23, ZSM-35 and mixtures thereof. The reactor used for dewaxing the relatively heavy chargestock contains a crystalline aluminosilicate zeolite having pore openings defined by: (1) a ratio of sorption of n-hexane to o-xylene, on a volume percent basis, or less than 3, which sorption is determined at a P/P.sub.o of 0.1 and at a temperature of 50.degree. C. for n-hexane and 80.degree. C. for o-xylene, (2) the abiilty of selectively cracking 3-methylpentane (3MP) in preference to the doubly branched 2,3-dimethylbutane (DMB) at 1000.degree. F. and 1 atmosphere pressure from a 1/1/1 weight ratio mixture of n-hexane/3-methyl-pentane/2,3-dimethylbutane, with the ratio of rate constants k.sub.3MP /K.sub.DMB determined at a temperature of 1000.degree. F. being less than about 2, and (3) a Constraint Index value of greater than about 1, e.g., ZSM-5, ZSM-11, ZSM-5/ZSM-11 intermediate and mixtures thereof.

REFERENCES:
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patent: 4229282 (1980-10-01), Peters et al.
patent: 4292166 (1981-09-01), Gorring et al.
patent: 4372839 (1983-02-01), Oleck et al.
patent: 4388177 (1983-06-01), Bowes et al.
patent: 4414097 (1983-11-01), Chester et al.

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