Catalytic codimerization of norbornadiene with norbornene

Details Catalytic codimerization of norbornadiene with norbornene Catalytic codimerization of norbornadiene with norbornene

1978-08-14

1980-02-26

O'Keefe, Veronica

Chemistry of hydrocarbon compounds

Alicyclic compound synthesis

Polycyclic product

585 14, 585 22, 149120, C07C 1332

Patent

active

041906110

ABSTRACT:
Norbornadiene and nobornene are catalytically codimerized to the saturated exo-exo hexacyclic dimer of norbornadiene. Used is a three-component homogeneous catalytic system consisting of cobaltic or cobaltous acetylacetonate, 1,2-bisdiphenylphosphino ethane and an alkyl aluminum chloride. Resulting dimer can be used as a component of high energy fuel.

REFERENCES:
patent: 2875256 (1959-02-01), Hyman
Carbonaro, J. Org. Chem., 36, p. 1443, 1971.
Mitsudo et al., J. Chem. Soc. Chem. Com., pp. 772-773, 1976.
Hara et al., Tetrahedron, 22, pp. 95-100, 1966.
Cagill et al., J. Org. Chem., 31, p. 3938, 1966.
Greco et al., J. Org. Chem., 35, p. 271, 1970.

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