Capsule and elements for synthesised diamond production

Single-crystal – oriented-crystal – and epitaxy growth processes; – Apparatus

Reexamination Certificate

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C117S929000

Reexamination Certificate

active

08057597

ABSTRACT:
The present invention consists in obtaining, with the capsule described, a vertical gradient favorable for diamond growth that prevails over any radial gradient by means of heating discs placed at the ends of the heating area, which implies a considerable control over the growth conditions. More specifically, in regard to the rate of growth, it allows for a better control of the quality of large crystals. Another important novelty is to use a source of carbon with a special design formed by cylindrical and conical hollows (graphite, amorphous carbon, diamond or other) with a solvent metal with a number of gases that are introduced in the capsule.Also, a nitrogen scavenger is used to avoid the formation of nitrides, carbides and oxides that are harmful for the growth and that as a significant novelty is placed outside the reaction area.

REFERENCES:
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patent: 4632817 (1986-12-01), Yazu et al.
patent: 6030595 (2000-02-01), Sumiya et al.
Wakatsuki, et al. “Growth of Diamond with Zr-containing Molten Metal Solvents and Metal Elements as Incorporated Impurities,”Diamond and Related Materials,, vol. 8, pp. 1438-1440, 1999.
International Search Report issued in International Application No. PCT/EP2005/000462 dated Dec. 20, 2005.
International Preliminary Report on Patentability issued in International Application No. PCT/EP2005/000462.
Written Opinion issued in International Application No. PCT/EP2005/000462.

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