Measuring and testing – Gas analysis – Gas of combustion
Patent
1996-12-17
1998-11-10
Oda, Christine K.
Measuring and testing
Gas analysis
Gas of combustion
422 94, G01N 700
Patent
active
058346279
ABSTRACT:
A combustible gas sensor that uses a resistively heated, noble metal-coated, micromachined polycrystalline Si filament to calorimetrically detect the presence and concentration of combustible gases. The filaments tested to date are 2 .mu.m thick.times.10 .mu.m wide.times.100, 250, 500, or 1000 .mu.m-long polycrystalline Si; some are overcoated with a 0.25 .mu.m-thick protective CVD Si.sub.3 N.sub.4 layer. A thin catalytic Pt film was deposited by CVD from the precursor Pt(acac).sub.2 onto microfilaments resistively heated to approximately 500.degree. C.; Pt deposits only on the hot filament. Using a constant-resistance-mode feedback circuit, Pt-coated filaments operating at ca. 300.degree. C. (35 mW input power) respond linearly, in terms of the change in supply current required to maintain constant resistance (temperature), to H.sub.2 concentrations between 100 ppm and 1% in an 80/20 N.sub.2 /O.sub.2 mixture. Other catalytic materials can also be used.
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Huber Robert J.
Hughes Robert C.
Manginell Ronald P.
Moreno Daniel J.
Ricco Antonio J.
Cone Gregory A.
Oda Christine K.
Politzer Jay L.
Sandia Corporation
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