Bromine removal from acetic acid

Distillation: processes – separatory – With chemical reaction – Including step of adding catalyst or reacting material

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Details

203 33, 203 37, 562414, 562549, 562608, B01D 300, C07C 5144, C07C 5308

Patent

active

042279712

ABSTRACT:
Concentrated acetic acid of 95 to 100 weight percent concentration containing both ionic and coordinate bromine can be successfully purified to a bromine content of less than 3 ppm by the sequential steps of catalytic hydrogenation, contacting the resulting acetic acid with alkali metal hydroxide, carbonate or bicarbonate, and then distilling acetic acid from the alkali metal.

REFERENCES:
patent: 2884451 (1959-04-01), Graham
patent: 3084109 (1963-04-01), Ure et al.

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