Boron removal from ethylene glycol-magnesium chloride solutions

Chemistry of inorganic compounds – Halogen or compound thereof – Binary compound containing metal

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423498, 260462R, C01F 530

Patent

active

042017580

ABSTRACT:
A method for removing boric acid and salts therefrom from ethylene glycol-magnesium chloride solutions which contain at least 100 ppm of boron which comprises reducing the pH of such solutions below 7 and then adding thereto at least 3 moles of methanol based on the amount of boric acid or salt thereof present in said solution and then subjecting the thus-treated ethylene glycol-magnesium chloride solution to distillation at a temperature sufficient to remove trimethyl borate-methanol therefrom, thereby reducing the level of boron in the starting solution to not more than 35 ppm.

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