Borate crosslinker suspensions with more consistent...

Earth boring – well treating – and oil field chemistry – Well treating – Contains inorganic component other than water or clay

Reexamination Certificate

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C507S922000, C507S903000

Reexamination Certificate

active

06936575

ABSTRACT:
The invention provides an aqueous suspension/concentrate of a sparingly soluble borate, preferably as disclosed in Mondshine U.S. Pat. No. 4,619,776, which is effective in crosslinking aqueous solutions of a water soluble, borate-crosslinkable polymer, preferably guar gum and derivatives thereof. The aqueous suspension/concentrate comprises a saturated aqueous solution of a sparingly soluble borate, a suspension agent, suspended particles of a sparingly soluble borate, and optionally a stabilizing agent, wherein the saturated solution of the sparingly soluble borate is prepared prior to the particles of the sparingly soluble borate being suspended therein. The preferred suspension agent is a palygorskite clay such as attapulgite and sepiolite. The invention further provides a method of hydraulically fracturing a formation with the aqueous borate suspension/concentrate.

REFERENCES:
patent: 2773757 (1956-12-01), Connell et al.
patent: 4619776 (1986-10-01), Mondshine
patent: 4620596 (1986-11-01), Mondshine
patent: 5565513 (1996-10-01), Kinsey et al.
patent: 2003/0144154 (2003-07-01), Dobson et al.

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