Benzene-tricarboxylic acid-(1,3,5)-tri-N-chloramide and process

Details Benzene-tricarboxylic acid-(1,3,5)-tri-N-chloramide and process Benzene-tricarboxylic acid-(1,3,5)-tri-N-chloramide and process

1977-04-28

1978-10-31

Douglas, Winston A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C10324, C07C 3910

Patent

active

041234618

ABSTRACT:
Phloroglucinol is prepared by chlorinating benzenetricarboxylic acid-(1,3,5)-triamide in an aqueous, inorganic acid medium to form benzene-tricarboxylic acid-(1,3,5)-tri-N-chloramide, which is a new compound; the latter is converted by treatment with ammonia into 1,3,5-triureido-benzene, which is hydrolyzed in inorganic acid solution to phloroglucinol.

REFERENCES:
Zabicky, "The Chemistry of Amides", p. 776 (1970).

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