Batch thermolytic distillation of carbonaceous material

Distillation: apparatus – Apparatus – Types

Reexamination Certificate

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Details

C202S262000, C202S117000, C202S118000, C202S119000, C202S103000, C202S108000, C422S268000, C422S269000, C422S270000, C422S271000

Reexamination Certificate

active

07056422

ABSTRACT:
A distillation system is provided for batch thermolytic distillation of lump carbonaceous material, such as lump wood and shredded rubber tires. The system preferably includes multiple distillation units mounted side-by-side. Each unit includes a reactor bath for holding molten tin at approximately 455° C., a two-compartment reservoir for storing molten tin, and a porous basket pivotally mounted within the reactor bath for tipping motion. A process for batch thermolytic distillation of lump carbonaceous material includes rotating the porous basket into a reactor bath by rotating the basket about an axis passing through the reactor bath; putting a charge of wood into the basket; closing a retractable lid onto the reactor bath; filling the reactor bath with molten material to produce gas and char by thermolytic conversion of the charge, draining the reactor bath of molten material while the lid is closed; quenching the char in the reactor bath with steam; opening the lid; and tipping the char from the basket.

REFERENCES:
patent: 4508564 (1985-04-01), Kennedy
patent: 4614752 (1986-09-01), Fuchs et al.
patent: 4925532 (1990-05-01), Meuser et al.
patent: 5449438 (1995-09-01), Jagau et al.
patent: 5852062 (1998-12-01), Carpenter
patent: 6051110 (2000-04-01), Dell'Orfano et al.
patent: 6346221 (2002-02-01), Wagner

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