Baked color pencil lead manufactured by impregnation with perhyd

Plastic and nonmetallic article shaping or treating: processes – Carbonizing to form article

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264 295, 264 296, 264 297, 264 41, 264 44, 264 459, 264 78, 264 82, 264 83, 264 85, 523164, C01B 3100

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057334820

ABSTRACT:
By kneading a composition containing a filler and an organic forming binder, extruding the composition, baking the composition in a non-oxidizing atmosphere, there is obtained a first baked lead containing, as a binder, a carbon obtained by the carbonization of the organic forming binder. Then, by heating the first baked lead in an oxidizing atmosphere to remove the binder carbon, there is formed a second baked lead composed of at least the filler. The pores of the second baked lead are impregnated with a solution containing perhydropolysilazane, subjecting the lead to a heat treatment in an inert atmosphere or an ammonia gas atmosphere to form a third baked lead containing the resultant silicon nitride. Finally, ink is filled into the pores of the third baked lead to provide a baked color pencil lead.

REFERENCES:
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patent: 3446878 (1969-05-01), Tsukahara
patent: 3592883 (1971-07-01), Kawakubo
patent: 4535007 (1985-08-01), Cannady
patent: 4543344 (1985-09-01), Cannady
patent: 4847345 (1989-07-01), Takamizawa et al.
patent: 4869854 (1989-09-01), Takeda et al.
patent: 5030702 (1991-07-01), Vaahs et al.
patent: 5595589 (1997-01-01), Hoshiba et al.
Database WPI, Week 8939, Derwent Publications Ltd., London, GB; AN 89-280942 & JP-A-01 203 476 (Toa Nenryo Kogyo KK), 16 Aug. 1989 (Abstract only).

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