Apparatus for the manufacture of a thermostable amorphous ferrom

Details Apparatus for the manufacture of a thermostable amorphous ferrom Apparatus for the manufacture of a thermostable amorphous ferrom

1988-03-23

1990-01-16

Rutledge, L. Dewayne

Metallurgical apparatus

Means for melting or vaporizing metal or treating liquefied...

By stirring or mixing molten metal

266234, 42218601, 432 75, C21C 700

Patent

active

048937932

ABSTRACT:
The thermostable amorphous ferromagnetic powder containing iron, cobalt, or nickel, also comprises xylene from 0.2 to 25% by volume of the powder particles, up to 20% chrome and boron by weight, and lithium or magnesium in amounts from 0.1 to 2.0% by weight. The powder is resistant to oxidizing up to temperatures of 250.degree. C. and has a specific surface up to 160m.sup.2 /g.
The method for its manufacture comprises reduction of a solution containing salts of iron, cobalt, chrome, a complexing agent, and metal salts or polyvalent alcohols by means of a reductant sodium borohydride in the presence of sodium hydroxide. The solution is protected by an organic hydrophobic substance--xylene during a period from 5 seconds to 10 minutes in the presence of a magnetic field.
The device for manufacture of the thermostable amorphous ferromagnetic powder comprises a vertical reactor with a stirrer and electromagnet generating a magnetic field. The reactor is cylindrical with a movable bottom and tubes are oriented vertically to the bottom. The reaction vessel is connected by two overflow tubes to an expanded collecting vessel. Both vessels have belts for shower jet washing with water for discontinuation of the reaction and after its cessation.
The ferromagnetic powder is used in the manufacture of magnetic media recording on disks, tapes and cards, etc.

REFERENCES:
patent: 4141763 (1979-02-01), Aonuma et al.
patent: 4294435 (1981-10-01), Matsuno
patent: 4445919 (1984-05-01), Cole et al.

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