Apparatus for removing pyrophoric catalyst

Liquid purification or separation – Filter – Within flow line or flow line connected close casing

Reexamination Certificate

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Details

C210S241000, C210S451000, C210S477000, C210S478000

Reexamination Certificate

active

06886698

ABSTRACT:
Spent pyrophoric reaction catalyst from a reaction mixture is removed safely, cheaply, and rapidly using a single plate pressure filter. After hydrogenation, the reaction mixture is decanted, the desired hydrogenation product is removed, and catalyst-rich material which settles at the bottom of the vessel is delivered to a single plate pressure filter fitted with a filter bag40of permeable material. The spent catalyst is retained in the filter bag40and stored under water awaiting recovery. The filter apparatus1comprises a container having a domed base2, a generally cylindrical sidewall3terminating in an upper rim4closed by a lid5having lifting lugs6. The lid5is fixed in pressure-tight engagement with the sidewall3by flange engaging screw clamps7and an embedded polytetrafluoroethene gasket8. The filter bag40is held in position by a band11and may be readily released for removal of the spent catalyst material. The bag40may be reused.

REFERENCES:
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patent: 4664798 (1987-05-01), Bergh
patent: 5690836 (1997-11-01), Raskin et al.
patent: 5840188 (1998-11-01), Kirsgalvis
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patent: 197 27 715 (1999-01-01), None
patent: 0 605 363 (1996-06-01), None
patent: WO 0143863 (2001-06-01), None
PCT International Search Report for PCT/IE00/00156.
PCT International Search Report for PCT/1E00/00155.

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