Apparatus for reacting a particulate solid and a liquid

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – With means applying electromagnetic wave energy or...

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422227, 422231, 422234, 423320, B01F 312, B01J 810, B01J 1918, B01J 1926

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043637868

ABSTRACT:
An apparatus useful for the preparation of phosphoric acid from phosphate rock and a strong acid, comprises a closed vessel, a draft tube, means connected to the inner walls of said vessel amd mounting said draft tube in a vertical position within said vessel, an agitator positioned within said draft tube, a shaft for said agitator mounted axially of said vessel and extending into said draft tube, an inlet conduit to said vessel for introducing a feed slurry (e.g. phosphate rock and strong acid) into said vessel, said inlet conduit preferably having a lower end portion terminating within said draft tube and wherein, said draft tube has an outwardly flared lower skirt portion terminating in the bottom portion of said vessel, and preferably including a vent pipe connected to said inlet conduit to reduce foaming generated by the reaction in said vessel and to prevent blockage of said inlet conduit, and including means for applying air, under pressure, to the bottom of said reactor and/or under the bottom of said lower skirt portion, to prevent settling of undissolved solids.

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