Apparatus for producing single crystal and quasi-single...

Single-crystal – oriented-crystal – and epitaxy growth processes; – Apparatus – For crystallization from liquid or supercritical state

Reexamination Certificate

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C117S081000, C117S083000, C117S213000

Reexamination Certificate

active

07368015

ABSTRACT:
An apparatus including a crucible, an energy source, and a controller is provided. The crucible may be sealed to a nitrogen-containing gas, and may be chemically inert to at least ammonia at a temperature in a range of about 400 degrees Celsius to about 2500 degrees Celsius. The energy source may supply thermal energy to the crucible. The controller may control the energy source to selectively direct sufficient thermal energy to a predefined first volume within the crucible to attain and maintain a temperature in the first volume to be in a range of from about 400 degrees Celsius to about 2500 degrees Celsius. The thermal energy may be sufficient to initiate, sustain, or both initiate and sustain growth of a crystal in the first volume. The first temperature in the first volume may be controllable separately from a second temperature in another volume within the crucible. The first temperature and the second temperature differ from each other. Associated methods are provided.

REFERENCES:
patent: 1879278 (1932-09-01), Jacobs
patent: 1986196 (1935-01-01), Grosse
patent: 2544414 (1951-03-01), Bridgman et al.
patent: 2745713 (1956-05-01), Suits
patent: 2785058 (1957-03-01), Buehler
patent: 2895812 (1959-07-01), Kohman
patent: 2941241 (1960-06-01), Strong
patent: 2947609 (1960-08-01), Strong
patent: 2947610 (1960-08-01), Hall et al.
patent: 3013867 (1961-12-01), Sawyer
patent: 3030662 (1962-04-01), Strong
patent: 3088170 (1963-05-01), Strong
patent: 3101259 (1963-08-01), Sawyer
patent: 3107395 (1963-10-01), Bundy
patent: 3313004 (1967-04-01), Vahldiek et al.
patent: 3473935 (1969-10-01), Wilson et al.
patent: 3567364 (1971-03-01), Flanigen et al.
patent: 3607014 (1971-09-01), Huml et al.
patent: 3650823 (1972-03-01), Mead et al.
patent: 3913212 (1975-10-01), Bachmann et al.
patent: 3933573 (1976-01-01), Dugger
patent: 4055982 (1977-11-01), Ter-Minassian et al.
patent: 4202930 (1980-05-01), Kokta et al.
patent: 4430051 (1984-02-01), von Platen
patent: 4523478 (1985-06-01), Zacharias, Jr.
patent: 4685995 (1987-08-01), Hirano
patent: 4699084 (1987-10-01), Wilson et al.
patent: 4762823 (1988-08-01), Watanabe et al.
patent: 4891165 (1990-01-01), Suthanthiran
patent: 4910403 (1990-03-01), Kilham et al.
patent: 4961823 (1990-10-01), Hirano et al.
patent: 5236674 (1993-08-01), Frushour
patent: 5868837 (1999-02-01), DiSalvo et al.
patent: 5902396 (1999-05-01), Purdy
patent: 5911824 (1999-06-01), Hammond et al.
patent: 5942148 (1999-08-01), Preston
patent: 5993545 (1999-11-01), Lupton et al.
patent: 6113985 (2000-09-01), Suscavage et al.
patent: 6177057 (2001-01-01), Purdy
patent: 6270569 (2001-08-01), Shibata et al.
patent: 6273948 (2001-08-01), Porowski et al.
patent: 6285010 (2001-09-01), Fujikawa et al.
patent: 6375446 (2002-04-01), Leonelli, Jr.
patent: 6398867 (2002-06-01), D'Evelyn et al.
patent: 6406540 (2002-06-01), Harris et al.
patent: 6592663 (2003-07-01), Sarayama et al.
patent: 6676752 (2004-01-01), Suscavage et al.
patent: 6692568 (2004-02-01), Cuomo et al.
patent: 6848458 (2005-02-01), Shrinivasan et al.
patent: 6861130 (2005-03-01), D'Evelyn et al.
patent: 2002/0122757 (2002-09-01), Chung et al.
patent: 2003/0041602 (2003-03-01), Williams, III et al.
patent: 2003/0066800 (2003-04-01), Saim et al.
patent: 2003/0127337 (2003-07-01), Hanson et al.
patent: 2003/0140845 (2003-07-01), D'Evelyn
patent: 2003/0141301 (2003-07-01), D'Evelyn et al.
patent: 2003/0164138 (2003-09-01), Sarayama et al.
patent: 2003/0183155 (2003-10-01), D'Evelyn et al.
patent: 2003/0209191 (2003-11-01), Purdy
patent: 2004/0003495 (2004-01-01), Xu
patent: 2004/0134415 (2004-07-01), D'Evelyn et al.
patent: 2005/0103257 (2005-05-01), Xu et al.
patent: 44 13 423 (1995-10-01), None
patent: 0 152 726 (1985-08-01), None
patent: 0 157 393 (1985-10-01), None
patent: 0 220 462 (1987-05-01), None
patent: 0 860 182 (1998-08-01), None
patent: 1 275 127 (1961-11-01), None
patent: 1 306 951 (1962-10-01), None
patent: 2 796 657 (2001-01-01), None
patent: 9 226 19 (1963-04-01), None
patent: 2 333 521 (1999-07-01), None
patent: 60091062 (1985-05-01), None
patent: 60122797 (1985-07-01), None
patent: 09206582 (1997-08-01), None
patent: 10005572 (1998-01-01), None
patent: 11060394 (1999-03-01), None
patent: 2001058900 (2001-03-01), None
patent: 20030176197 (2003-06-01), None
patent: 2004066108 (2004-04-01), None
patent: WO 98/55671 (1998-12-01), None
patent: WO 01/24921 (2001-04-01), None
patent: WO 01/36080 (2001-05-01), None
patent: WO 02/34972 (2002-05-01), None
patent: WO 03/064021 (2003-08-01), None
patent: WO 2004/053206 (2004-06-01), None
patent: WO 2004/053208 (2004-06-01), None
patent: WO 2004/071649 (2004-08-01), None
patent: WO 2005/122232 (2005-12-01), None
K. Byrappa and Masahiro Yoshimura, “Apparatus”, Handbook of Hydrothermal Technology, pp. 82-160, 2001.
Dissertation: Cubic Boron Nitride: Stability of the Domain and new Ways of Elaboration, Translated from French by the Ralph McElroy Co., Custom Division, PO Box 4828, Austin, Texas 78765 USA.
H. Jacobs et al, “High Pressure Ammonolysis in Solid-State Chemistry”, Materials Science, vol. 8, Chapter 5, pp. 383-427, 1982.
V. L. Solozhenko et al., “On The Lowest Pressure of Sphaleritic Boron Nitride Spontaneous Crystallization”, J. Superhand Maker, vol. 14, No. 6, Letters to the Editor, Allerton Press, Inc., p. 64, 1992.
Mark A. Sneeringer et al, “Milk Cartons and Ash Cans: Two Unconventional Welding Techniques”, American Mineralogist, vol. 70, pp. 200-201, 1985.
ES Itskevich, “High-Pressure Cells for Studies of Properties of Solids(Review)”, Instruments and Experimental Techniques, vol. 42, No. 3, pp. 291-302, 1999.
Scott L. Boetttcher, “A Simple Device for Loading Gases In High-Pressure Experiments”, American Mineralogist, vol. 74, pp. 1383-1384, 1989.
Andrew D. Hanser et al, “Growth, Doping and Characterization of Epitaxial Thin Films and Patterned Structures of A1N, GaN, and A1xGa1-xN”, Diamond and Related Materials, vol. 8, pp. 288-294, 1999.
K. Lawniczak-Jablonska et al., “Polarization Dependent X-Ray Absorption Studies of the Chemical Bonds Anisotropy in Wurtzite GaN Grown at Different Conditions”, Journal of Alloys and Compounds, vol. 328, pp. 77-83, 2001.
Zhong Weizhuo, “Synthetic Crystallization”, (2ndEdition, Scientific Publication Press, ISBN 7-03-003952-1/O 689, 2 pages, Oct. 1994.
M. Bickermann et al, “Characterization of Bulk AIN With Low Oxygen Content”, Journal of Crystal Growth, vol. 269, pp. 432-442, 2004.
M. Yano et al., “Growth of Nitride Crystals, BN, A1N and GaN By Using a Na Flux”, Diamond and Related Materials, Elsevier Science Publishers, Amsterdam, NL, vol. 9, No. 3-6, pp. 512-515, Apr. 2000.
Masaichi Yano et al., “Control of Nucleation Site and Growth Orientation of Bulk GaN Crystals”, Japanese Journal of Applied Physics, Publication Office Japanese Journal of Applied Physics, Tokyo, Japan, vol. 38, No. 10A, Part 2, pp. L1121-L1123, Oct. 1, 1999.
Joseph W. Kolis et al., “Materials Chemistry and Bulk Crystal Growth of Group III Nitrides in Supercritical Ammonia”, Materials Research Society, vol. 495, pp. 367-372, 1998.
Masato Aoki et al., “Growth of 5 mm GaN Single Crystals at 750° C. From An Na-Ga Melt”, American Chemical Society, Crystal Growth & Design, vol. 1, No. 2, pp. 119-122, Feb. 3, 2001.
S. Porowski, “Near Defect Free GaN Substrates”, High Pressure Research Center, Polish Academy of Sciences, Sokolowska 29/37, 01-142 Warsaw, Poland, sylvek@unipress.waw.pl, 11 pages, 1999.
S. Porowski et al., “Growth of GaN single Crystals Under High Nitrogen Pressure”, High Pressure Research Center, Polish Academy of Sciences, ul. Sokolowska 29/37, 01-142, Warsaw, Poland, Chapter 9, pp. 295-313, 1997.

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