Apparatus for producing aromatic dicarboxylic acids

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – Including solid – extended surface – fluid contact reaction...

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422226, 422231, 422235, 422236, 422240, 261 93, 261 97, 261122, 562416, 562410, 562414, B01J 810, C07C 6314

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active

041593073

ABSTRACT:
An apparatus for producing an aromatic dicarboxylic acid by oxidizing a benzene derivative with molecular oxygen in the liquid phase in a lower aliphatic carboxylic acid as a solvent in the presence of an oxidation catalyst, wherein a starting material liquid e.g., a benzene derivative or a solution thereof in the lower aliphatic carboxylic acid, is fed into the liquid-phase reaction system in a uniformly dispersed state by being passed through a porous material causing the pressure of the starting material liquid just after passing through said porous material to drop more than about 1 kg/m.sup.2 in relation to the pressure of the starting material liquid just before passing through said porous material. The resultant aromatic dicarboxylic acid has high purity and has good color.

REFERENCES:
patent: 3093626 (1963-06-01), Cines
patent: 3407179 (1968-10-01), Carr
patent: 3677714 (1972-07-01), Ledgett
patent: 3721530 (1973-03-01), Bouchet
patent: 4062654 (1977-12-01), Shigeyasu et al.

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